Efficient validation strategies in environmental analytical chemistry: A focus on organic micropollutants in water samples

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• dc.contributor.author Hernández, Félix
• dc.contributor.author Fabregat-Safont, David
• dc.contributor.author Campos-Mañas, Marina
• dc.contributor.author Quintana, José Benito
• dc.date.accessioned 2024-02-21T07:16:03Z
• dc.date.available 2024-02-21T07:16:03Z
• dc.date.issued 2023
• dc.description.abstract This article critically reviews analytical method validation and quality control applied to the environmental chemistry field. The review focuses on the determination of organic micropollutants (OMPs), specifically emerging contaminants and pesticides, in the aquatic environment. The analytical technique considered is (gas and liquid) chromatography coupled to mass spectrometry (MS), including high-resolution MS for wide-scope screening purposes. An analysis of current research practices outlined in the literature has been performed, and key issues and analytical challenges are identified and critically discussed. It is worth emphasizing the lack of specific guidelines applied to environmental analytical chemistry and the minimal regulation of OMPs in waters, which greatly affect method development and performance, requirements for method validation, and the subsequent application to samples. Finally, a proposal is made for method validation and data reporting, which can be understood as starting points for further discussion with specialists in environmental analytical chemistry.
• dc.description.sponsorship The authors from University Jaume I acknowledge financial support from Generalitat Valenciana (Research Group of Excellence Prometeo 2019/040) and Ministerio de Ciencia e Innovación (Ref. PID2021-127451OB-I00). J.B.Q. acknowledges funding provided by Xunta de Galicia (Ref. ED431C 2021/06), the Spanish Agencia Estatal de Investigación – MCIN/AEI/10.13039/501100011033 (Ref. PID2020-117686RB-C32).
• dc.format.mimetype application/pdf
• dc.identifier.citation Hernández F, Fabregat-Safont D, Campos-Mañas M, Quintana JB. Efficient validation strategies in environmental analytical chemistry: A focus on organic micropollutants in water samples. Annu Rev Anal Chem (Palo Alto Calif). 2023 Jun 14;16(1):401-28. DOI: 10.1146/annurev-anchem-091222-112115
• dc.identifier.doi http://dx.doi.org/10.1146/annurev-anchem-091222-112115
• dc.identifier.issn 1936-1327
• dc.identifier.uri http://hdl.handle.net/10230/59201
• dc.language.iso eng
• dc.publisher Annual Reviews Inc
• dc.relation.ispartof Annu Rev Anal Chem (Palo Alto Calif). 2023 Jun 14;16(1):401-28
• dc.relation.projectID info:eu-repo/grantAgreement/ES/3PE/PID2021-127451OB-I00
• dc.relation.projectID info:eu-repo/grantAgreement/ES/2PE/PID2020-117686RB-C32
• dc.rights © 2023 by the author(s). This work is licensed under a Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. See credit lines of images or other third-party material in this article for license information.
• dc.rights.accessRights info:eu-repo/semantics/openAccess
• dc.rights.uri http://creativecommons.org/licenses/by/4.0/
• dc.subject.keyword Liquid and gas chromatography
• dc.subject.keyword Mass spectrometry
• dc.subject.keyword Method validation
• dc.subject.keyword Organic micropollutants
• dc.subject.keyword Quality assurance and quality control
• dc.subject.keyword Water
• dc.title Efficient validation strategies in environmental analytical chemistry: A focus on organic micropollutants in water samples
• dc.type info:eu-repo/semantics/article
• dc.type.version info:eu-repo/semantics/publishedVersion